1H-benzo[b]azepine
7-Chloro-1,2,3,4-tetrahydro-1-(2-methyl-4-nitrobenzoyl)-5H-1-benzazepin-5-one
CAS: 137982-91-3
Molecular Formula: C18H15ClN2O4
1H-benzo[b]azepine - Names and Identifiers
1H-benzo[b]azepine - Physico-chemical Properties
| Molecular Formula | C18H15ClN2O4 |
| Molar Mass | 358.78 |
| Density | 1.387 |
| Melting Point | 152 - 155°C |
| Boling Point | 573.3±50.0 °C(Predicted) |
| Solubility | DMSO (Slightly), Methanol (Slightly) |
| Appearance | Solid |
| Color | White to Off-White |
| pKa | -2.58±0.20(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
1H-benzo[b]azepine - Introduction
7-Chloro-1, 2,3, 4-tetrahydro -1-(2-methyl-4-nitrobenzoyl)-5H-1-benzazepin-5-one, also known as N-nitro-5-one chloride. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
-Appearance: White crystalline solid
-Molecular formula: C13H12ClN3O4
-Molecular weight: 319.71g/mol
-melting point: 136-138 ℃
-Soluble: Soluble in ethanol, benzene and dichloromethane, insoluble in water
Use:
-7-Chloro-1, 2,3, 4-tetrahydro -1-(2-methyl -4-nitrobenzoyl)-5H-1-benzazepine-5-one is an important organic synthesis Intermediate, commonly used in the preparation of active molecules in pesticides and pharmaceuticals.
-It can be used as a raw material for pesticides, herbicides and fungicides, and can also be used to synthesize some drugs, such as antibiotics and anti-cancer drugs.
Preparation Method:
-7-Chloro-1, 2,3, 4-tetrahydro -1-(2-methyl-4-nitrobenzoyl)-5H-1-benzazepine-5-one can be prepared by chlorinating 4-nitroanisole with 1,2, 3,4-tetrahydro-1-benzazepine-5-one in the presence of ferric chloride.
Safety Information:
-7-chloro-1, 2,3, 4-tetrahydro -1-(2-methyl -4-nitrobenzoyl)-5H-1-benzazepine-5-one is an organic compound with certain toxicity and irritation.
-Wear appropriate protective equipment such as protective gloves, goggles and face shields during handling and handling.
-Avoid contact with skin and eyes, avoid inhaling its vapor or dust.
-When storing, it should be stored in a sealed container, away from fire and oxidizing agents.
-When using or handling this compound, follow local safe operating procedures.
Nature:
-Appearance: White crystalline solid
-Molecular formula: C13H12ClN3O4
-Molecular weight: 319.71g/mol
-melting point: 136-138 ℃
-Soluble: Soluble in ethanol, benzene and dichloromethane, insoluble in water
Use:
-7-Chloro-1, 2,3, 4-tetrahydro -1-(2-methyl -4-nitrobenzoyl)-5H-1-benzazepine-5-one is an important organic synthesis Intermediate, commonly used in the preparation of active molecules in pesticides and pharmaceuticals.
-It can be used as a raw material for pesticides, herbicides and fungicides, and can also be used to synthesize some drugs, such as antibiotics and anti-cancer drugs.
Preparation Method:
-7-Chloro-1, 2,3, 4-tetrahydro -1-(2-methyl-4-nitrobenzoyl)-5H-1-benzazepine-5-one can be prepared by chlorinating 4-nitroanisole with 1,2, 3,4-tetrahydro-1-benzazepine-5-one in the presence of ferric chloride.
Safety Information:
-7-chloro-1, 2,3, 4-tetrahydro -1-(2-methyl -4-nitrobenzoyl)-5H-1-benzazepine-5-one is an organic compound with certain toxicity and irritation.
-Wear appropriate protective equipment such as protective gloves, goggles and face shields during handling and handling.
-Avoid contact with skin and eyes, avoid inhaling its vapor or dust.
-When storing, it should be stored in a sealed container, away from fire and oxidizing agents.
-When using or handling this compound, follow local safe operating procedures.
Last Update：2024-04-09 02:00:42
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